GC/MS analysis results for sample AD23473, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23473.D Vial: 4 Acq On : 16 Oct 2001 5:10 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Hexatriacontane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 35.50 4.32 ug/1 438469 Perylene-dl2 37.23 Hit# Of 5 Tentative ID MW MolForm CAS# Qual (^^Hexatriacontane 507 C36H74 000630-06-8 94 2 Heneicosane 296 C21H44 000629-94-7 91 3 Tetracosane 338 C24H50 000646-31-1 90 4 Nonacosane ____________________ 408 C29H60 000630-03-5 90 Abundance Scan 3318 (35.498 min): 23473.D (-) m/z 57.00 100.00% 57 71 43 5000 85

I 99 A I r' • ' I 35.20 35.40 35.60 35.80 m/z TIToO 72.72%

I TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Hexatriacontane 43 57

71 5000 85 35.20 35.40 35,60 35.80 m/z 43.00 64.04% ____ Il _x21215LL£! 155169183197211 pnrVryHHTT^pT-T-ryrVTTYTTT-Vp-rTTp-TTT^ I' ' ' ' I ' ' ‘' I' '' ' I ' ' '' I r ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #4220tHeneioosane _ '517 __ _ ) 71 85 35.20 35.40 35.60 35.80 5000 m/z 85.05 49.30% 99

tJLm I ' 'TH IVI I I I I I I• 268 296 {'' ' ' I' ' ' ' I I " " 1" '' I' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane ............ /...................... 35.20 35.40 35.60 35.80 ~71 m/z 41.00 22.20% 5000 85

• 99 J I''' ' I l| T 155169183197 294 338 ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.20 35.40 35.60 35.80

23473.D NP091101.M Wed Oct 17 13:17:53 2001 Page 15

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