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GCMS analysis comments for sample AD28664, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting TurboVap contamination and recovery data for sample AD28664.

NYC-WTC_000035115–000035134

Folder label: “GCMS X 11/24/01 A 12/4/01

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Scanned page image, NYC-WTC_000035130
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0401\28664.D Vial: 18 Acq On 5 Dec 2001 4:58 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heneicosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 32.66 0.66 ug/1 151784 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 90 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 87 3 Heptadecane, 9-hexyl- 324 C23H48 055124-79-3 87 4 Pentacosane 352 C25H52 000629-99-2 87 Abundance Scan 3008 (32.657 min): 28664.D (-) m/z 57.00 100.00% 57 43 71 85 5000 ------------ 99 32.40 32.60 32.30 33.00 1 J 113127141 155 169183196 211 281 TTTTd rj TTTTT H rip tn | t i* i i p i < I । i H i । i i i i । i i i i । i i i i |* i i i i । i i TTTTT m/z 43.05 72.24% miz-2 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42201: Heneicosane 57 71 85 5000 i . I i i i t-j- > > > > |Trrr] । । 32.40 32.60 32.80 33.00 99 m/z 71.10 69.69%

m/z- .... 4 1 ,........................... . ।, ....... 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #50999: Eicosane. 7-hexyl- 43 57 -P — i ■ — -PP 71 32.40 32.60 32.80 33.00 5000 85 m/z 85.05 53.05%

. 99 113127141 169182 197 281 310 ■ ■ ■ i' ■1 ■ i ■ TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT miz-2 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance 43 57 #46162: Heptadecane, 9-hexyl- —....... 4A''— 32.40 32.60 32.80 33.00 m/z 41.05 27.87% 71 5000 85

210 99 113 127 141 296 324 I 239 T"tEII"IEIT"EETTITTII-"III1" AY.A4—-MPI 111 ■ ■ 1 1,1 ' 1 ‘ 1 1 1 | 1 > • 'T 1 ' n | I I M p . . . | . I |« m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 32.40 32.60 32.80 33.00

28664.D GCMS1126.M Fri Dec 07 15:54:09 2001 Page 7

NYC-WTC_000035130

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NYC-WTC_000035130Source: NYC Law Department, mirrored locally

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