GCMS analysis results for sample AD28430, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28430 .D vial: 12 Acq On 4 Dec 2001 11:06 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 MisC : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Heneicosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 29.55 0.93 ug/1 231968 Chrysene-dl2 33.04 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7( 91 2 Octadecane 254 C18H38 000593-45-3 91 3 Eicosane 282 C20H42 000112-95-8 90 4 Tetracosane ___________________________ 338 C24H50 000646-31-1 87 Abundance Scan 2670 (29.552 min): 28430.D (-) m/z 57.00 100.00% 57

43 71 5000 85

99 11." ' I 1 ' ■ ' i 1 29.20 29.40 29.60 29.80 0-- +127141 155169183197211—— 253 310 ■ ■ i ■ ■ ■' i " " i' ■ ■ ■ i ■ ■ ■ ■ i m/z 71.00 65.48% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 71 85 5000 ‘I f |Tr ■ ■ | ■ 29.20 29.40 29.60 29.80 99 m/z 43.00 63.55% — b J 113127 141 155 -------- 268 296 T’I I ' 11 * I 1 1 1 1 1 1 ' ' 'I 11 '' ' I ' ' ‘11 ' ' ' ' I mfz~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71560: Octadecane 43 57 ............ .........................................

71 29.20 29.40 29.60 29.80 5000 85 m/z 85.00 47.59%

99 — IJI I 113127141 169 183 197210 254 I F I TTTT , I ( I , I'! I I f | I ri , T’mau, ■ ■ ■ i ■ ■ mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #39862: Eicosane "I" 43 5 7 29.20 29.40 29.60 29.80 71 m/z41.05 30.92%

5000 85

99 113127141155 196 240 282 TIT "E" - — —PPP i -IT m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

28430.D GCMS1126.M Wed Dec 05 08:19:35 2001 Page 2

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