GCMS analysis results for sample AD28430, Dec 2001

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Library Search Compound Report Data File : C: \HPCHEM\1\DATA\DEC0401\28430.D Vial: 12 Acq On : 4 Dec 2001 11:06 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.44 8.04 ug/1 002520 Chrysene-d12 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl hexadecanoate 312 C20H40O2: oooooo-oo-o 53 2 Cyclobutane, 1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 3 l-Hexene, 2-methyl- 98 C7H14 006094-02-6 27 4 Cycloheptyl line 113 C7H15N 005452-35-7 27 Abundance Scan 2658 (29.442 min): 28430.D (-) m/z 56.00 100.00%

5000 4'

1. 73 101 129 239 257 —... J — —.... 29.20 29.40 29.60 29.80

n/z-> " I" TIIr 711 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 1015717112519212 4 283 , 312 m/z 57.00 48.48% Abundance #44549: Butyl hexadecanoate 55

5000 258 T 29.20 29.40 29.60 29.80 73 240 312 m/z 43.05 40.88% 129

m/z-> 20 40 60 4144— TU—nngr ■ ■ i ■ ■ 157171135 214 —..... — 80 100 120 140 160 180 200 220 240 260 280 300

AA Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- 55 ' 1 l ' ' 29.20 29.40 29.60 29.80 5000 m/z 41.05 38.32%

27 70 ■ ■ । I >i■ 97 111125 140 168 196........... miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261:1-Hexene, 2-methyl- 55 ■ ■ i ■ ' ' I 1 '1 • I ' ’ 29.20 29.40 29.60 29.80 m/z 55.00 32.65% 41 5000 27 70

m/z—> 20 40 60 1 98 80 100 120 140 160 180 200 220 240 260 280 300 ,. — .. LL A 29.20 29.40 29.60 29.80

28430.D GCMS1126.M Wed Dec 05 08:19:33 2001 Page 1

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