GCMS blank analysis for sample AD28662, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0401\28662.D vial: 15 Acq On 5 Dec 2001 2:02 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.44 4.78 ug/1 1028180 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl hexade anoate 312 C20H40O21 000000-00-0 35 2 Cyclobutane l,l-dimethyl-2-octyl- 196 C14H28 062338-30-1 35 3 1-Hexene, 2 -methyl- 98 C7H14 006094-02-6 27 4 Pentadecane, 8-methyl ene- 224 C16H32 055668-09-2 25 Abundance Scan 2657 (29.436 min): 28662. D (-) m/z 56.00 100.00% 55

5000 41 73 257 T 129 239 ■ ‘ ■ i 29.20 29.40 29.60 29.80 ■ ■ ■ i' TT40 I Me ; ,87 10115 143157171185199213 4 "TTTTTT’TTTT’TT TT’ , T ’I ’ ’’0 r, TTTTT TT । 283,312 m/z 57.00 48.92% m&-> 20 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 55

5000 240 258 312 -.— — A r 29.20 29.40 29.60 29.80 73 129 m/z 41.05 40.48%

miz-> " 1111'1111 20 40 60 I 1911 1 TIPupmg 157171185 214 .—..m 80 100 120 140 160 180 200 220 240 260 280 300 TT Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- 55 T TT TT TT T 29.20 29.40 29.60 29.80 5000 m/z 43.05 40.44% __

27 70 — ■ ■ i " '' i " 'r r .97111125 140 168 196 nlz~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261:1-Hexene, 2-methyl- 1 1 I ' 55 29.20 29.40 29.60 29.80 m/z 55.00 29.79% 41 5000 27 70 98 || ■' r' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ' 1 1 r 1 r1-1 T • I ■ ' 1 ■ i 1 • m/z—> 20 29.20 29.40 29.60 29.80

28662.D GCMS1126.M Thu Dec 06 13:20:02 2001 Page 1

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