GCMS analysis comments for sample AD28669, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC0401\28692.D Vial: 19 Acq On 5 Dec 2001 5:56 am Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.44 6.95 ug/1 - 1229910 Chrysene-dl2 33.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual l Butyl hexadecanoate 312 C20H40O21 000000-00-0 35 2 1-Hexene, ethyl- 2- 98 C7H14 006094-02-6 27 3 Cyclobutane 1,l-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 4 1-Pentene,^2,4-dimethy1- 98 C7H14 002213-32-3 27 Abundance Scan 2657 (29.438 min): 28692.D (-) m/z 56.00 100.00% 55

5000 41 73 257 . —PPP 101 129 239 ' 1 1 1 ’ 11J + J. 7 4lE 1, 143157171185199213/ 4 283,. 1 312 . m/z 29,20 29.40 29.60 29.80 57.00 48.39% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 55

5000 73 240 312 m/z —. LU ■ i ■ ■ 29.20 29.40 29.60 29.80 43.05 40.42% 129

mz—> 20 4 _11—1...157171185 214 40 60 — ------ TT‘ 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261:1-Hexene, 2-methyl- 55 • • । ■ —A 29.20 29.40 29.60 29.80 41 m/z 41.05 38.58% 5000 27 70 | 98 mfz~> 20 40 60 "sb" 100 120 140 160 180 200 220' 240 260 280 3007 Abundance #21985: Cyclobutane, 1,1 -dimethyl-2-octyl- P1. 11 — 55 29 20 29.40 29.60 29.80 m/z 55.00 30.52% 5000

27 70 97 111125 140 — ।...I . । IIr. ri, 168 196 m , 11.1. | .... । < 1., ।,.. , । ..,. ।., t q । iii । 11 11 11 M 11 । in 11 TI m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

28692.D GCMS1126.M Thu Dec 06 12:39:25 2001 Page 1

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