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GC/MS analysis results for sample AD23272, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.

NYC-WTC_000088456–000088484

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088467
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23272.D Vial: 22 Acq On : 12 Oct 2001 10:39 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 5 Butyl hexadecanoate Concentration Rank 1 R.T. EstCbnc Area Relative to ISTD R.T. 29.51 9.02 ug/1 965628 Chrysene-dl2 33.12 Hit# of 5 fentative ID MW MolForm CAS# Qual

1 Butyl he^decanoate 312 C20H4 0O2: 000000-00-0 53 2 1-Hexei^ 2-methyl- 98 C7H14 006094-02-6 27 3 Cyclobutane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 4 Oxir^e, 2,3-bis (1-methylethyl)t 128 C8H16O 054644-32-5 23 Abundance Scan 2666 (29.512 min): 23272.D (-) Tm/z 56.00 100.00% 53

5000 41 73 257 101 ' 239 29.20 29.40 29.60 29.80 , J I. -1-^^57171185^99213 | '' i'' " I'' m/z 57700 46.61% ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 53

258 r-r-rr-r-r-r-rXA/-W>^^ 5000 I 2a20 29^40 2a60 2a80 73 240 312 m/z 129 43.00 36.18% I I 157171^?^ . i I '■ I I . 'i r j . I . I I rn i* |-i-. V 1 j .... I I I I rj- I'''•I n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300

—JUx- Abundance #63261:1-Hexene, 2-methyl- 53 1 29.20 29.40 29.60 29.80 41 m/z4170535.27% 5000 27 70 I 98 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 /Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- r, n-< ,'Tr rr-ij 53 29.20 29,40 29,60 29.80 m/z 73.00 28.89%

27 70 U-44 I 9/ 111125140 168 196 I '”’”'' I' p-n-r-p-r-n-j- /1 ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23272.D NP091101.M Mon Oct 15 09:41:58 2001 Page 5

1 NYC-WTC_000088467"

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