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GC/MS calibration data sheet for October 5, 2001

Machine-extracted title · confidence 90%

Laboratory data sheet listing extraction dates and calibration results for deuterated standards.

NYC-WTC_000087980–000087999

Folder label: “GC/MS Scan 9/24/01

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NYC 9/11 Public Portal Document

Library Search Compound'Report

Data File : C:\HPCHEM\1\DATA\OCT0401\LB.D Vial: 9 Acq On : 4 Oct 2001 11:22 pm Operator: 209 GALOS Sample : 9/24 Inst : GC/MS 209 Mise - Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Butyl hexadecanoate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

29.54 2.58 ug/1 445362 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hexai^canoate 312 C20H40O2 000000-00-0 40 2 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 27 3 Cyclobu^ .ne, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 4 Oxi ran;/, 2,3-bis(1-methylethyl)-, t 128..C8H16O 054644-32-5 23 Abundance / Scan 2668 (29.536 min): LB.D (-) m/z 56.00 100.00% 56

5000 41 ^29 239 T ■n-''" I 312 29;20 2940 29t0 2^ pnrHT m/z 57.00 46.21% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate

258 M. △ 5000 29^0 29.40 29.60 29.80 73 312 116129 m/z 41.0.5 37.61% I 157171185 214 p/z-> 20 ........ 11""!.' VYTr^VlYrTHnqT-T-T-TYr-rW-ph-rTq-rT^^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #1354; 1-Hexene, 2-methyl- 56 ! MJ0 29,40 29t0 29J0 5000 V I m/z 43.0„5 ■ 37.27% 27 : I 70 , 83 ............... m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- , I j-r Ti , I I I 'Ti , I 5(6 29.20 29.40 29.60 29.80 m/z 73.0.0 28.93% 5000

27 70 83 |\ 97 111 125140 168 196 . ........... I ' ' ' ' I I ' ' ' ' I ' ' ' ' I -n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

LB.D NP091101.M Tue Oct 09 12:50:23 2001 Page 3

NYC-WTC_OO6o87988

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NYC-WTC_000087988Source: NYC Law Department, mirrored locally

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