Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On : 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample : 9/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Butyl hexadecanoate Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T. 29.54 2.04 ug/1 329818 Chrysene-dl2 ■ 33.16
Hit# Of 5 Tent ve ID MW MolForm CAS# Qual
1 Butyl hexadepanoate 312 C20H40O2 000000-00-0 32 2 1-Hexene, 2^methyl- 98 C7H14 006094-02-6 27 3 Cyclobutahe, 1,l-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 4 1,3 -I^2^nediol, 2-ethyl- 146 C8H18O2 000094-96-2 25 Abundance Scan 2668 (29.537 min): LBE.D (-) m/z 56.00 100.00%
5000 41 73
, i III 129 I 1431571711^1992^ 257 A M ....... 29.20 29.40 29.60 29.80 312 'i ' I I ' I ' ' ' I I ' I I ' I m/z 57.00 47744% mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 55
5000 258 29.20 29.40 29.60 29.80 240 312 m/z 129 43.00 36.99% . 1 I I . I I I I I I I r I . . I I I I . I I I I I . . J . . I I |-| ri I I
mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300
Ma Abundance #1354:1-Hexene, 2-methyl- 53
29.20 29.40 29.60 29.80 n 41 5000 m/z 41.05 36.94% 27 70 98 J '''' I' I " '' I''' ‘ I " '' I'' ’' I''' ’ I ■ ’" I'' " I "T ■n/z-> 20 40 60 80 100 120 140-160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- T 55 29.20 29,40 29.60 29.80 Wz 73,00 31.89%
Mia I 27 70 I I L 9/ 111125140 168 196 rTVT7^‘TTnYrT+-rp-rT-T-|T-TT^^ I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' H ' ’ ' ' I Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80
LBE.D NP091101.M Wed Oct 03 14:41:12 2001 Page 8
NYC-WTC_000087145
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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