Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample 9/18 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 1,4-Dichlorobenzene-d4 Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 11.64 0.54 ug/1 75603 1,4-Dichlorobenzene-d4 11.78
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 1,4-Dichlor5^nzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1/2\ 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzaldefiyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 Benzo/hran, 7-chloro- _________________ 152 C8H5C1O 024410-55-7 9 Abundance < Scan 719(11.644 min): LBE.D (-) m/z 149.90 100.00% 1!i0
5000 115 , ,, , I , , , , I -n ,/ I . I 1 . I . . . 52 78 38 45 11.40 11.60 11.80 12.00 ,1 m/z 151.90 61791% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene<l4 1!i0
5000 115 78 11.40 11.60 11.80 12.00 52 m/z 114.90 32.31% 35 ' I ' ■■
m/z-> 30 40 50 60 70 80 90 100 11012gi30 140 150 1OT Abundance #9592: Benzene-1.2,3.4-d4-, 5,6-dichloro- 1!i0 L 11.40 11.60 11.80 12.00 115 5000 52 78 m/z 77.95 . 17.65%
35 87 I I ' ' I ' ' ' ' I ' ' ' ' I P"' ' ' I ' ‘ I ' ' ' ' I ' ' ' I ' ' ' ' I ' ' nfe-> Abundance 30 40 50 60 70 80 90 100 110 120 130 #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 140 150
152 160 L 11.40 11.60 11.80 12.00 T
m/z 52.00 14.95% 106 5000 53 81
122 ' I'''' I'''' I' ' I ' 92 4UX 136 I ' I ' ' ' ' I ' ' ' ' I T ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00
LBE.D NP091101.M Wed Oct 03 14:41:10 2001 Page 7
NYC-WTC_000087144
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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