Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On : 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample : 9/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P
Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Pentanone Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 10.84 0.44 ug/1 60964 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentamone 86 C5H10O 000107-87-9 53 2 2-Buta: !ne, 3-methyl- 86 C5H10O 000563-80-4 50 3 Acetip- acid ethenyl ester 86 C4H6O2 000108-05-4 37 4 2,3 -^tanedione 86 C4H6O2 000431-03-8 9 ^bundance"^^^ Scan 631 (10.837 min): LBE.D (-) m/z 42.95 100700% 4)3
5000
tVz-> Abundance 58
...................... I" " 96 !5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 #62837:2-Pentanone I" " I' 86
m/z X 10.60 10.80 11.00 11.20 58.05 22.96%
4^
A 5000 10.60 10.80 11.00 11.20 27 57 86 m/z 85.95 18.79% 71 A..... r "' I' I ‘ I" " I"'' 11 ‘' I I"" Ti/z-> 5 10.15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #703:2-Butanone, 3-methyl- 4)3
''' I'' I ' ' ' ' I ' ' 10.60 10.80 11.00 11.20 5000 m/z 41.05 9.99% 27 86 38 I 57 71 pTTTjjrTTJTTTTpTTTpT^ +r T Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #62795: Acetic acid ethenyl ester 4^ 10.60 10.80 11.00 11.20 m/z71.00 8.34% 5000
86
tt/z-> ..... 5 I..... +t I " ' ' I " " I " '' I " " I " " I 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 JSUV ' ' i ' 10.60 10.80 11.00 11.20
LBE.D NP091i01.M Wed Oct 03 14:41:08 2001 Page 6
*NYC-'WTC_000087i 43
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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Technical form recording liquid-liquid extraction parameters including drip rates and pH measurements for WTC samples.
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Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.
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NYC-WTC_000087044
Laboratory report documenting GC/MS analysis of sample AD22550 conducted on September 27, 2001, identifying unknown compounds.
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