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GCMS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 90%

Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.

NYC-WTC_000068559–000068571

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\LB.D Vial: 2 Acq On : 5 Nov 2001 12:14 pm Operator: 209 GALOS Sample : 10/16 lab blk Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanol, 4-methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.68 0.45 ug/1 79598 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanol, -methyl- 102 C6H14O 000108-11-2 83 2 2-Hexanol 102 C6H14O 000626-93-7 83 3 2-Butam 74 C4H10O 000078-92-2 56 4 2-Buta: 1, 74 C4H10O 015892-23-6 50 Abundance Scan 178 (6.676 min): LB.D (-) m/z 44.95 100.00% 4)5

5000

69 6.40 6.60 6.80 7.00

□u 51 87 . .............. II.... ....... 98 I" ‘' I m/z 69.00 14.76% Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63546: 2-Pentanol, 4-methyl- 4)5

5000 6.40 6.60 6.80 7.00 "m/z 417700“ 11.94% 27 69

lU_ 57 I 87 . ..................... ............................ "I I' " ' I" " I tt/2-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63584: 2-Hexanol 4|5

u 6.40 6.60 6.80 7.00 5000 m/z 44.00 11.13%

69 87 ....”.............. ■|"H|'I..| p-n-rp-rT-rf 1'' “ I Ti/z->10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #62568:2-Butanol 4)5 6.40 6.60 6.80 7.00 m/z 43100 9104%

5000

31

Tiyz~> ....... X..I . . 7 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 72 '' 1'' " I' " ' I" '' I' 6.40 6.60 6.80 7.00

LB.D NP103001.M Fri Nov 09 12:14:16 2001 Page 3

NYC-WTC_000068567

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NYC-WTC_000068567Source: NYC Law Department, mirrored locally

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