Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
NYC-WTC_000068559–000068571Folder label: “508 Scan X 10/16/01 A 11/5/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\LB.D Vial: 2 Acq On : 5 Nov 2001 12:14 pm Operator: 209 GALOS Sample ; 10/16 lab blk Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C;\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.77 ug/1 137218 1,4-Dichlorobenzene-d4 11.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 91 2 2-Hexap;one, 4-hydroxy-5-methyl-3-pr 172 C10H20O2i 061141-74-0 83 3 2-He3c^one, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 72 4 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 Abundance Scan 151 (6.428 min): LB.D (-) m/z 42 795 100.00% 43
58 5000
71 85 100 6.00 6.20 6.40 6.60 6.80 49 , ,li . ....I, I I I , , , [-1 , , , I I............. , '■'V m/z 58.05 51.90% Ti^-> 20 30 40 50 6o 7o 8g 9o jiog jiio ji2g j3O jL^ Abundance #63387; 2-Hexanone
58 5000 6.00 6.20 6.40■ 6.60 6.80 100 m/z 41.05 18.30% 71 85 ' p ' ' ''i ' ' ' ' I ' ... l''.... '' I' 'nh.-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #15807:2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 4)3
6.00 6.20 6.40 6.60 6.80 5000 Wz 57.00 16.46% 58 27 85 100 I ' I ' ' ' ' I ' ' ' ‘ p Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 i'W Abundance #11968; 2-Hexanone, 4-hydroxy-3-propyl- 43 6.00 6.20 ‘ ' 6.^ ' ' 6.^ 6.80 m/z 100.00 11.98% 58 5000 29
,1 ' I ' ' ’ 71 I 85 4 100 .-.-.. ... 140 Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 6.60 6.80
LB.D NP103001.M Fri Nov 09 12:14:14 2001 Page 2
NYC-WTC_000068566
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NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Log sheet recording liquid-liquid extraction parameters and sample processing details for November 2001.
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Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.
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