GC/MS TCLP calibration table analysis, October 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\LB.D Vial: 3 Acq On : 15 Oct 2001 1:28 pm Operator: 209 GALOS Sample : lab blk 9/28 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.95 ug/1 104679 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone/^ 100 C6H12O 000591-78-6 91 2 Methyl I/obutyl Ketone 100 C6H12O 000108-10-1 58 3 2-Hexa^ne, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 53 4 2-Hep^none, 7,7-dichloro- 182 C7H12C12O 000000-00-0 53 Abundance Scan 156 (6.476 min): LB.D (-) m/z 42.95 100.00% 4(3

58 5000

100 6.20 6.40 6.60 6.80 53 I 71 85 . .................. . ........ I""l..... m/z 58.05 61.91% ■nlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556:2-Hexanone 43

58 5000 6,20 6,40 6,60 6.80 ~m7z 41.05 15.90% 27 85 71 100 •r<Tr.|.ll*p."l4-ni............................. I......... ■r+-T TTfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ikbundance __ #63354: Methyl Isobutyl Ketone ............. .

__a2D__&4p_6;60_a80^_ 5000 m/z 57.00 15.75% 58

85 100

Tl/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ... 1.: Abundance - -- #15807: 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- “±^4t3-------- ---------- priip—=- ' 6?^ " 6.60-Z Seo m/z 100.05 13777%

5000 58. -- 27- 72 I'' " I'''' I' I ' I'' ,| 85 100 " JI'' I'''' I" '' I" " I " " I' " ' I " " I" '' I TlZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

LB.D NP091101.M Tue Oct 16 15:20:27 2001 Page 2

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