GC/MS analysis report with TCLP calibration table data from October 16, 2001.
NYC-WTC_000089030–000089044Folder label: “GC/MS Scan 9/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\LB.D Vial: 3 Acq On : 15 Oct 2001 1:28 pm Operator: 209 GALOS Sample : lab blk 9/28 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.95 ug/1 104679 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone/^ 100 C6H12O 000591-78-6 91 2 Methyl I/obutyl Ketone 100 C6H12O 000108-10-1 58 3 2-Hexa^ne, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 53 4 2-Hep^none, 7,7-dichloro- 182 C7H12C12O 000000-00-0 53 Abundance Scan 156 (6.476 min): LB.D (-) m/z 42.95 100.00% 4(3
58 5000
100 6.20 6.40 6.60 6.80 53 I 71 85 . .................. . ........ I""l..... m/z 58.05 61.91% ■nlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556:2-Hexanone 43
58 5000 6,20 6,40 6,60 6.80 ~m7z 41.05 15.90% 27 85 71 100 •r<Tr.|.ll*p."l4-ni............................. I......... ■r+-T TTfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ikbundance __ #63354: Methyl Isobutyl Ketone ............. .
__a2D__&4p_6;60_a80^_ 5000 m/z 57.00 15.75% 58
85 100
Tl/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ... 1.: Abundance - -- #15807: 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- “±^4t3-------- ---------- priip—=- ' 6?^ " 6.60-Z Seo m/z 100.05 13777%
5000 58. -- 27- 72 I'' " I'''' I' I ' I'' ,| 85 100 " JI'' I'''' I" '' I" " I " " I' " ' I " " I" '' I TlZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80
LB.D NP091101.M Tue Oct 16 15:20:27 2001 Page 2
NYC-WTC_000089037
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NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087496
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000089025
Fragmented GC/MS scan page from a laboratory blank sample dated September 28, 2001.
Filed in the same folder
NYC-WTC_000089026
Fragmented GC/MS scan page from a laboratory blank sample dated September 28, 2001.
Filed in the same folder
NYC-WTC_000089045
Laboratory report documenting GC/MS analysis of sample AD23652 conducted on October 16, 2001.
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NYC-WTC_000089059
Laboratory report documenting GC/MS analysis of sample AD23651 conducted on October 16, 2001.
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NYC-WTC_000089073
Laboratory record for sample AD23653 showing detection of unknown compounds on October 16, 2001.
Filed in the same folder