GC/MS TCLP calibration table analysis, October 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\LB.D Vial: 3 Acq On : 15 Oct 2001 1:28 pm Operator: 209 GALOS Sample : lab blk 9/28 Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

6.60 0.46 ug/1 50899 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 Tentative ID Z-' MW MolForm CAS# Qual ■

1 3-Hexanol 102 C6H14O 000623-37-0 78 2 Silane, tirimethyl- 74 C3H10Si 000993-07-7 53 3 3-Penta nol, 2-methyl- 102 C6H14O 000565-67-3 45 4 Octant 7-hydroxy-3,7-dimethyl- 172 C10H20O2 000107-75-5 36 Abundance Scan 170 6.604 min): LB.D (-) “m/z 59705 100.00% 5P

5000 73

43 100 6.20 6.40 6.60 6.80 7.00 .......I|lili|..fi! Hill........ Ill 84 ........ m/z 55.00 83.86% TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529; 3-Hexanol 5b

31 553 73 ' I ' ' ' ' I ' ' 6.20 6.40 6.60 6.80 ZOO in/z 73.00 48.26% 44 rrp-rrq-rl-rr|-t-r.i pi-I i p-l i l | i . m । i i i 102 11 1111'l i i i । i 11 i । i I 11 । i i i i 11 i i . , i rn । i rr i । i i 11 [I??. । i i i . । .

■nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #331: Silane, trimethyl- 5b ■

73 6.^ 6.40 6.60 6.80 7.00 5000 m/z 43.05 23.93%

45 I

Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance---- - - — #63561:3-Pentanol, 2-methyl- ■ ' ~ ” II. Il ■ I <11 ■ I • —A .. I« ab« I - »- — — I . — —

-6.20-216.40—6:60^6:80” 7.00- “m/z 41.05 15.32%

5000- 73

31 45 I'''' I 4 85 102 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80 7.00

LB.D NP091101.M Tue Oct 16 15:20:29 2001 Page 3

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