GC/MS calibration table, Oct 2001

NYC 9/11 Public Portal Document , . ^Quantitation Report (QT Reviewed) Data File : C : \HPCHEM\l\DATA\OCTOigi\LBC>^3(<>2/n l/Z} 0 Vial: 3 Acq On : 1 Oct 2001 3:40 pm I • Operator: 209 GALOS Inst : GC/MS 209 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 2 12:07 2001 Quant Results File: NP091101.REE Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Thu Sep 13 12:47:04 2001 I . Response via : Initial Calibration / /)\ DataAcq Meth : NP091101 // /\

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.79 152 568247 20.00 ug/1 -0.12 19) Naphthalene-d8 15.40 136 2250370 20.00 ug/1 -0.12 31) Acenaphthene-dlO 20.69 164 1091866 20.00 ug/1 -0.12 49) Phenanthrene-dlO 25.12 188 1555767 20.00 ug/1 -0.12 59) Chrysene-dl2 33.16 240 1140813 20.00 ug/1 -0.12 68) Perylene-dl2 37.28 264 844008 20.00 ug/1 -0.14 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.78 132 240 0.01 ug/1 0.37 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.30 152 6437 0.23 ug/1 -0.13 Spiked Amount 50.000 Recovery = 0.46% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.84 172 2499 0.03 ug/1 0.03 Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 30.02 244 215 0.00 ug/1 -0.13 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 5.14 79 181 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(l-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration LBC.D NP091101.M Tue Oct 02 12:07:34 2001 Page 1

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