GC/MS calibration table for TCLP analysis, Nov 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\NOV0801\LBA.D ry’ Vial: 8 Acq On ; 8 Nov 2001 9 : 26 pm ‘, J Operator: 209 GALOS Sample : 10/19 lab blk 0 s Inst : GC/MS 209 Mise : Q/oJO-- ' Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 8 22:15 2001 Quant Results File: NP103001.RES Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Nov 02 16:41:16 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.72 152 1290885 20.00 ug/1 0.00 19) Naphthalene-d8 15.32 136 4940198 20.00 ug/1 0.00 31) Acenaphthene-dlO 20.60 164 2456399 20.00 ug/1 0.00 49) Phenanthrene-dlO 25.03 188 3625376 20.00 ug/1 0.00 59) Chrysene-dl2 33.07 240 2679409 20.00 ug/1 0.00 68) Perylene-dl2 37.17 264 2171791 20.00 ug/1 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.72 132 1155 0.01 ug/1 0.48 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.23 152 13735 0.23 ug/1 -0.02 Spiked Amount 50.000 Recovery = 0.46% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.74 172 5564 0.04 ug/1 0.12 Spiked Amount 50.000 Recovery = 0.08% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration LBA.D NP103001.M Mon Nov 19 15:54:25 2001 Page 1

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