Header page for a gas chromatography-mass spectrometry scan file related to environmental testing at the World Trade Center site.
NYC-WTC_000030685–000030697Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) 1535-o go Data File : C:\HPCHEM\1\DATA\NOV1901\LBA.D 7S 7* *— 7 ) Vial: 14 Acq On Sample : 20 Nov 2001 : gc/ms unknown 3:59 am 29973—7 /I n 7% 0 1 507- 11 Operator: Inst : 209 GALOS GC/MS 209 ___ Mise : 2. ) 1 Multiplr: 1.00 MS Integration Params: RTEINT.P 260)% Quant Time: Nov 20 4:48 2001 258% Quant Results File: NP103001.RES
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Nov 02 16:41:16 2001 Response via : Initial Calibration DataAcq Meth : NP103001
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.72 152 708815 20.00 ug/1 0.00 19) Naphthalene-d8 15.31 136 2666181 20.00 ug/1 -0.02 31) Acenaphthene-diO 20.59 164 1311673 20.00 ug/1 -0.02 49) Phenanthrene-diO 25.02 188 1951201 20.00 ug/1 -0.02 59) Chrysene-dl2 33.05 240 1471211 20.00 ug/1 -0.02 68) Perylene-dl2 37.15 264 1088589 20.00 ug/1 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.72 132 490 0.01 ug/1 0.48 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.25 152 838 0.03 ug/1 0.00 Spiked Amount 50.000 Recovery = 0.06% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.75 172 1519 0.02 ug/1 0.13 Spiked Amount 50.000 Recovery = 0.04% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00%
Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D.
(#) = qualifier out of range (m) = manual integration LBA.D NP103001.M Mon Dec 10 14:50:20 2001 Page 1
NYC-WTC_000030685
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NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033886
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069215
Laboratory report documenting GCMS analysis of sample AD25038 conducted on November 19, 2001, noting violations and unknown compounds.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069644
Laboratory report documenting GCMS analysis of sample AD25460 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069659
Laboratory report documenting GCMS analysis of sample AD25461 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068413
Laboratory report documenting GCMS analysis of sample AD24431 conducted on November 7-9, 2001, identifying unknown compounds.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Gas chromatography-mass spectrometry scan record from late October to November 2001 regarding environmental sample analysis.
Filed in the same folder
NYC-WTC_000030680
Chromatogram and calibration data for DFTPP standard used to verify GC/MS instrument performance during environmental analysis.
Filed in the same folder
NYC-WTC_000030698
Gas chromatography-mass spectrometry analysis of sample AD25845, December 12, 2001, identifying other unknown compounds with threshold of 5.0 ug.
Filed in the same folder
NYC-WTC_000030708
Laboratory report documenting GCMS analysis of sample AD25873 conducted on December 12, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000030719
Laboratory commentary on GCMS scan of sample AD25874 dated December 13, 2001, identifying tetrachloroethane and noting a blank analysis.
Filed in the same folder