Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
NYC-WTC_000068230–000068239Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV0101\LBA.D Vial: 8 Acq On ; 1 Nov 2001 9:51 pm , Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 5 13:23 2001 Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901
Internal Standards R.T, Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.71 152 556018 20.00 ug/1 -0.02 19) Naphthalene-d8 15.32 136 2199501 20.00 ug/1 -0.02 31) Acenaphthene-dlO 20.60 164 1069558 20.00 ug/1 -0.02 49) Phenanthrene-dlO 25.02 188 1582117 20.00 ug/1 -0.02 59) Chrysene-dl2 33.05 240 1122672 20.00 ug/1 -0.02 68) Perylene-dl2 37.16 264 803738 20.00 ug/1 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.72 132 301 0.01 ug/1 0.48 Spiked Amount 75.000 Recovery 0.01% 7) 1,2-Dichlorobenzene-d4 12.23 152 6241 0L30^g/l -0.02 Spiked Amount 50.000 Recovery 0.60% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.74 172 2331 0.04 ug/1 0.12 Spiked Amount 50.000 Recovery = 0.08% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recoveiry = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. {#) = qualifier out of range (m) = manual integration LBA.D NP103001.M Wed Nov 07 14:57:08 2001 Page 1
NYC-WTC_000068230
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NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031054
Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031350
Calibration data table for gas chromatography-mass spectrometry analysis dated December 3, 2001.
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NYC-WTC_000068224
Record of a GCMS scan conducted at the World Trade Center site in early November 2001.
Filed in the same folder
NYC-WTC_000068225
Laboratory note regarding trace detection of 1,2-Dichlorobenzene-d4 in multiple samples attributed to laboratory contamination.
Filed in the same folder
NYC-WTC_000068240
Laboratory report documenting GCMS analysis of environmental sample AD24334 with detection of unknown compounds.
Filed in the same folder
NYC-WTC_000068255
Laboratory report documenting GCMS analysis of environmental sample AD24335 with detection of unknown compounds.
Filed in the same folder
NYC-WTC_000068266
Laboratory report documenting GCMS analysis of environmental sample AD24395 with detection of unknown compounds.
Filed in the same folder