Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
NYC-WTC_000031054–000031062Folder label: “GCMS X 11/2/01 A 12/1/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
« Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV3001\LBE.D Vial: 52 Acq On : 30 Nov 2001 Operator: 209 GALOS Sample : lb 11/2 gc/ms 4'40 P 26)04 Inst : GC/MS 209 Mise MS Integration Params: RTEINT.P —008 Multiplr: 1.00 Quant Time: Nov 30 17:31 2001 Quant Results File: NP112601.RES Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 09:03:50 2001 Response via : Initial Calibration DataAcq Meth : NP112601
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.70 152 929893 20.00 ug/1 0.00 19) Naphthalene-d8 15.30 136 3567591 20.00 ug/1 0.00 31) Acenaphthene-diO 20.58 164 1690363 20.00 ug/1 0.00 49) Phenanthrene-diO 25.00 188 2351640 20.00 ug/1 0.00 59) Chrysene-dl2 33.03 240 1483668 20.00 ug/1 0.00 68) Perylene-dl2 37.13 264 1080496 20.00 ug/1 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.70 132 807 .01 ug/1 0.49 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.22 152 10817 0.28 ug/1 0.00 Spiked Amount 50.000 Recovery = 0.56% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.73 172 3660 0.04 ug/1 0.15 Spiked Amount 50.000 Recovery = 0.08% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 5.16 79 202 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2’ -oxybis (1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration LBE.D NP112601.M Mon Dec 03 09:14:17 2001 Page 1
NYC-WTC_000031054
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NYC-WTC_000030923
Calibration data for GC/MS analysis using Method 508 and TCLP procedures dated November 30, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070089
DEP laboratory report documenting GC/MS results for sample AD25830 analyzed on December 6, 2001.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069501
Calibration data table for GCMS analysis of compounds including naphthalene and phenanthrene from November 10, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000030966
Single-page GCMS document identifier from the Environmental Protection Department archive covering late 2001 testing records.
Filed in the same folder
NYC-WTC_000030967
Administrative record of GCIMS scanning operations for World Trade Center environmental samples between November and December 2001.
Filed in the same folder
NYC-WTC_000030969
Laboratory report documenting GCMS analysis of sample AD26129 conducted on December 3, 2001.
Filed in the same folder
NYC-WTC_000030980
Laboratory report documenting GCMS analysis of sample AD26128 conducted on December 3, 2001.
Filed in the same folder
NYC-WTC_000030992
Laboratory report documenting GCMS analysis of sample AD26130 conducted on December 3, 2001.
Filed in the same folder