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Method 608 sample preparation log, Dec 2001

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Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.

NYC-WTC_000031054–000031062

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document t

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV3001\LBE.D Vial: 52 Acq On : 30 NOV 2001 4:40 pm Operator: 209 GALOS Sample : lb 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 30 17:31 2001 Quant Results File: NP112601.RES Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 09:03:50 2001 Response via : Initial Calibration DataAcq Meth : NP112601

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 2 8) Naphthalene 15.37 128 415 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 3 8) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. 4 0) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 21.08 165 186 N.D. 45) Diethylphthalate 22.11 149 211 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 168 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachioropheno1 0.00 266 0 N.D. 5 5) Phenanthrene 24.99 178 822 N.D. 56) Anthracene 24.99 178 822 N.D. 57) Di-n-butylphthalate 27.01 149 4218 N.D. 5 8) Fluoranthene 0.00 202 0 N.D. 60) 3,31-Dichlorobenzidine 0.00 252 0 N.D. 61) Benzidine 0.00 184 0 N.D. 63) Pyrene 0.00 202 0 N.D. 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benzo(a)anthracene 33.03 228 3380 N.D. 66) Bis(2-ethylhexyl)phthalate 33.31 149 12212 N.D. 67) Chrysene 33.03 228 3380 N.D. 69) Di-n-Octylphthalate 0.00 149 0 N.D. 70) Benzo(b)fluoranthene 0.00 252 0 N.D. (#) = qualifier out of range (m) = manual integration LBE.D NP112601.M Mon Dec 03 09:14:22 2001 Page 2

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GCMS calibration table, Nov 2001 · Box DEP Box 21

NYC-WTC_000030923

Calibration data for GC/MS analysis using Method 508 and TCLP procedures dated November 30, 2001.

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