NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
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GC/MS calibration table for TCLP analysis, Oct 18 2001
Machine-extracted title · confidence 100%Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
NYC-WTC_000088491–000088503Folder label: “GC/MS Scan 9/26/01”
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NYC 9/11 Public Portal Document 1
Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT18 01\LB.D Vial: 2 Acq On : 18 Oct 2001 5:09 pm Operator: 209 GALOS Sample : lab blk 10/15 ' Inst : GC/MS 209 . MS Integration Params: RTEINT.P 3 A—- -A ^^1 -Multiplr: 1.00 Quant Time: Oct 19 9:49 2001 Qjant Results File; NP091101.RES Quant Method : C;\HPCHEM\l\METHODS\NP091101 .M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 ) Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.77 152 364582 20.00 ug/1 -0.14 19) Naphthalene-d8 15.37 136 1432838 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.66 164 675108 20.00 ug/1 -0.15 49) Phenanthrene-dlO 25.09 188 970393 20.00 ug/1 -0.15 59) Chrysene-dl2 33.12 240 727492 20.00 ug/1 -0.16 68) Perylene-dl2 37.23 264 524790 20.00 ug/1 -0.19 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 ’ 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.28 152 3766 0.21 ug/l -0.15 Spiked Amount 50.000 Recovery = 0.42% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery • = 0.00% 32) 2-Fluorobiphenyl 18.80 172 1419 0.03 ug/1 -0.01 Spiked Amount 50.000 Recovery = 0.06%. 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% . Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. k 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 .0 N.D. 18) Hexachloroethane 0.00 117. 0 N.D'. . 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 . 0. N.D. (#) = qualifier out of range (m) = manual integration LB.D NP091101.M Fri Oct 19 09:56:00 2001 Page. 1
NYC-WTC_000088491
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