DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
NYC-WTC_000067623–000067634Folder label: “GCMS Scan X 10/4/01 An 10/18/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\LBA.D vial: 11 Acq On : 17 Oct 2001 11:05 pm Operator: 209 GALOS Sample : lab blk 10/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.50 ug/1 49181 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 tative ID MW MolForm CAS# Qual 1 2-HexanojK 102 C6H14O 000626-93-7 78 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-HeXhnol, (R)- 102 C6H14O 026549-24-6 56 4 2-^^anol, (S) - 102 C6H14O 052019-78-0 56 e Scan 184 (6.733 min): LBA.D (-) m/z 45.00 100.00% 4)5
5000
69 51 56 I 87 6,40 6.60 6.80 7.00 98 I" "I"" I""H‘ ‘I m/z 41.05 16.13% n&-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1(X) 105 Abundance #63584:2-Hexanol 4)5
5000 6.40 6.60 6.80 7.00 m/z 69.10 15.53% ... ”...... T I, I,., 11,,,, I,,,, I,,, 11,1., I,,., I,,,, I,, I, I,,, 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1773:2-Pentanol. 4-methyl- 4)5 .. S.t... • • I ' ' ‘ ‘ I ' ' • • I I • / • I • • • • I 6.40 6.60 6,80 7.00 5000 m/z 43.05 14.65%
27 I" " I 'I" I' ‘" I ®7 T TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1794:2-Hexanol, (R)- 4)5 6.40 6.60 6.80 7.00 m/z 44.00 8.99% 5000
19 I?. . I 55_____ ? 87 ________ iyrrrTJTTTTyTTTTJTTTTylTTTYrrT4p4Tr|-|TTTTyrTTT^TTTTpTTTpTTTyrrrrpT7TpTTTyrrrTpTTTJTTTTpTTTyrT Tlfe-> 10 15 20253035404550556065 70 75 80859095 1QQ105 6.40 6.60 6.80 7.00
LBA.D NP101901.M Tue Oct 23 12:53:58 2001 Page 3
NYC-WTC_000067631
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NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031054
Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000067619
Record of a GCMS scan conducted at the World Trade Center site in early November 2001.
Filed in the same folder
NYC-WTC_000067620
Header page from a GCMS scan batch dated October 4, 2001, associated with DEP laboratory operations.
Filed in the same folder
NYC-WTC_000067635
DEP lab report for GCMS analysis of sample AD23915 conducted on October 25, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000067651
DEP lab report for GCMS analysis of sample AD23947 conducted on October 25, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000067675
DEP lab report for GCMS analysis of sample AD23948 conducted on October 25, 2001, noting unknown compounds.
Filed in the same folder