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GC/MS analysis results for sample AD22580, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22580 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087202–000087225

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087212
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22580.D Vial: 8 Acq On : 28 Sep 2001 7:17 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 6.75 0.63 ug/1 91579 1,4-Dichlorobenzene-d4 11.78 Hit# Of/ 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H14O 000626-93-7 83 2 ^Pentanol, 4-methyl- 102 C6H14O 000108-11-2 74 3/2-Butanol 74 C4H10O 000078-92-2 50 >4 2-Hexanol, (S) - 102 C6H14O 052019-78-0 43 /bundance Scan 186 (6.751 min): 22580.D (-) Wz 44.95 100.00% 40

5000

41 69 51 5,® 59 I 73 M87 640 6.60 6.80 7.00 ........................................................... . ................... m/z eTToT” 15.98% TT/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584; 2-Hexanol 40

5000 6.40 m/z 6.60 41.05 JU6.80 7.00 13.41% 69 19 27 31 4^1 I "I••■11• IIII " " 11 • • 11' I " I " 111' Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 'Msundance #63546: 2-Pentanol, 4-methyl- 415

640 6.60 6.80 7.00 5000 m/z 42.95 12.00%

27 69 4: 57 8487 19 I 3,1 ■n/z-> Abundance 10 111111"" 111" I *" 11 15 20 25 30 35 40 i+M ......... I" I---' 45 50 55 60 65 70 75 80 85 90 95 #62568:2-Butanol Aj VAw. ... ............... ... I I I '• I I 43 640 6.60 6.80 7.00 m/z 43.95 10.45% 5000

27 59 56 I T-rvrrfHA 72 ........................................................................ Tt-T-ry P" ■n^-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

22580.D NP091101.M Wed Oct 03 11:37:42 2001 Page 4

NYC-WTC_000087212

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NYC-WTC_000087212Source: NYC Law Department, mirrored locally

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