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GCMS analysis results for sample AD24473, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24473 conducted on November 9, 2001, identifying unknown compounds.

NYC-WTC_000068447–000068459

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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Scanned page image, NYC-WTC_000068456
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV0201\24473.D Vial: 17 Acq On : 3 Nov 2001 6:35 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.66 0.46 ug/1 62010 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanol 102 C6H14O 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 83 3 2-Hexanol, (R)- 102 C6H14O 026549-24-6 64 4 2-Hexanol, (S)- 102 C6H14O 052019-78-0 43 Abundance Scan 176 (6.657 min); 24473.D (-) m/z 44.90 100.00% 4)5

5000

41 69 50 53 __640_a60__a8p__Y0p__ 'I"'' ........... ................. .......................... m/z 41.05 15.87% Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63582; 2-Hexanol 43

5000 a40 a60 a80^w 27 m/ z; 69.00 14.86% 69 19 31 57 I 8487 XrrrTyrV^-r^TTin-p-rA-p-rrTYrrrT-^^^ n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63545; 2-Pentanol, 4-methyi- 4b

6.40 6,60 6.80 7.00 5000 m/z 43.00 12.23%

a 69 2,7 3942 I 57 8487

JJ I " " I " " I " " I' I " I " ' ‘ I " ' 11' III ......................."I ' I " ' 11' I " I " " I' TTfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1794; 2-Hexanol, (R)- 4l5 __64o__a6o__a8o__Aog^ m/z 44.00 9713% 5000

1^ 3942, 69 19 55 8487 I'''' 1' -p-rn-p-rrTp-rr Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

24473.D NP103001.M Tue Nov 13 11:53:51 2001 Page 2

NYC-WTC_000068456

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NYC-WTC_000068456Source: NYC Law Department, mirrored locally

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