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GCMS analysis results for sample AD24473, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24473 conducted on November 9, 2001, identifying unknown compounds.

NYC-WTC_000068447–000068459

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24473.D Vial: 17 Acq On : 3 Nov 2001 6:35 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 0.78 ug/1 104878 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 Morpholine, 4^methyl- 101 C5H11NO 000109-02-4 9 3 3 -Hydroxy- ^pentanone 102 C5H10O2 003142-66-3 9 4 2-Pentano^4 2,4-dimethyl- 116 C7H16O 000625-06-9 9 Abundance / Scan 289 (7.694 min): 24473.D (-) m/z 42.95 100.00% 4)3

59 5000

101

83 7.40 7.60 7.80 8.00 37, I I ' ' ' ' I ' ' ' ' I ''' ' ' I ' ' ' I I ' ' ' ' I ' m7z 59705 55.43% Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 4)3

5000 59 _740__Z60_^,80__a00__ m/z 100.95 22.98%

L, 15 31 101 I ' I ' "'n'" " I I 83 I ' I-'-'"I I I I ■ I ■ 1 I , I 1 1 I ■ I I . I I I I I I ■ I I I I I TlZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640; Morpholine, 4-methyl- 4)3 ' ' ' I ' ' ■ ' I ‘ ' 7.40 7.60 7.80 8.00 5000 m/z 58.05 20.94% 101 15 71 /l\ 27 II I I I I I56 I I I I I I I I p ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691: 3-Hydroxy-2-pentanone 31 59 7.40 7.60 7.80 8.00 m/z 41.00 8.34%

5000 45 15 , , I...... II...... I ' ‘ ' I ' ' ‘ ' I ' ' ' ' I ’l , . I , I , , . . , I , 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

24473.D NP103001.M Tue Nov 13 11:53:58 2001 Page 3

NYC-WTC_000068457

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NYC-WTC_000068457Source: NYC Law Department, mirrored locally

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