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GCMS analysis results for sample AD24946, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24946 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069084–000069094

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24946.D Vial: 14 Acq On : 7 Nov 2001 1:27 am Operator: 209 GALOS San^ile : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Librairy : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.06 ug/1 421727 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, #-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 56 2 Morpholine, X-methyl- 101 C5H11N0 000109-02-4 9 3 3-Hydroxy-^pentanone 102 C5H10O2 003142-66-3 9 4 Acetone / 58 C3H6O 000067-64-1 9 Abundance Scan 288 (7.692 min): 24946.D (-) m/z 42.95 100.00% -0 59 5000-

101 83 7.4o' ‘7.60' 7.M 's.oo' 39 I 69 I‘‘' I ' ‘ ‘ I ‘ ' 'I' I ■ ' ' ' I ' ■ ' ' I ‘ I ' • I I ( I • • • 1 ■ m/z 59.05 50.37% Tl/Z->

Abundance 10 20 30 40 50 60 70 80 #64274:2-Pentanone, 4-hydroxy-4-methyl- 90 100 110 1 5000 59 "7.46 7.60' 7.^ 8.06 m/z 101.05 21.61% 27 101 I I ,,|l, ,49,,.,.Hl,,. ' I ‘ ‘ 83 ' I ' ' ' ' I TiZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- -0 7.40 7.60 7.80 8.00 5000 m/z 58.05 17.95% 101

L 15 71 27 tVz-> MU 10 ’ ' '2® 30 I 56 I ' H ' ' ‘ I ' ' I ' I ' ' ' ' I ‘ 40 50 60 70 ‘ I ‘ ‘ 80 ' 1 ‘ ‘ 90 ' P ' ' ' 1 ‘ 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59 7.40 7.ro '7.^ 8.00 m/z 41.05 7.20% 5000

rJz-> 15 ..I......II...... I ,, 10 20 30 40 45

50 ||. .qs. 60 70 . .y.. 80 90 ... 100 .. 110 7.^' 7.ro L TT-r-p-r-r-r-j-r- 7.80 8.00

24946.D NP103001.M Pri Nov 16 14:57:20 2001 Page 1

NYC-WTC_000069092

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NYC-WTC_000069092Source: NYC Law Department, mirrored locally

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