GCMS analysis results for sample AD25262, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV0901\25262.D Vial: 12 Acq On : 9 Nov 2001 11:09 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 2.94 ug/1 462661 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanon^ 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 33 2 MorpholinX^ 4-methyl- 101 C5H11N0 000109-02-4 9 3 Acetone/ 58 C3H6O 000067-64-1 9 4 3-Hydro"^-2-pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 287 (7.682 min): 25262.D (-) m/z 43700 100.00% 4)3

59 5000

101 ,,,,,,,,,, J.. ..

.u 7.40 7.60 7.80 8,00 0^ ............. 38 I ' I ' ' ' ' I ' ' ‘ ' I ' ' ' ' I .-7-7.. HtT-TT-TYn-rT-r-p^T-rT-pT-T-H-r^t^^ 69 83 in/z 59705 51.74% nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 4)3

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 22.16% 27 101 ......... I I 83 '-r+ ' I ' ' ' ' I ' ' ' ■ I ''' ' ' I ' Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 4b J 7.4o' '7.60' '7.80' 'a.bo' 5000 m/z 58.05 177^1% 101 15 71 I —f—r-r-T-T—J— 27 -tVtn-n-n- I.. ....,1...... ■nA:-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone 43 7.40 7.60 7.80 8,00 m/z 41.00 6.84% 5000 58 27 . ..... ■*1'7 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

25262.D NP103001.M Tue Nov 27 12:29:07 2001 Page 1

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