GCMS analysis results for sample AD25947, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2101\25947.D Vial: 8 Acq On : 21 Nov 2001 6:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.73 3.89 ug/1 900931 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 -Pentanone, 44-hydroxy-4-methyl - 116 C6H1202 000123-42-2 72 2 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 3 Acetone 58 C3H60 000067-64-1 9 4 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 293 (7.731 min): 25947.D (-) m/z 43.0,0 100.00% 4)3

59 5000 101 TI1r > • • । ■ t ■ * TIT 1 T 69 83 , | 7.40 7.60 7.80 8.00 miz- -- 10 -- 20 .. 38. 30 40 fr 50 53+ — — 60 70 80 1T I 1 11 । ■ 1 i ■ 90 100 110 m/z 59.05 50.25% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 * * i ■ ' 1 * i ■1 * * 1 ; 1 TTTT ■ ‘ ■ ■ । 59 7.40 7.60 7.80 8.00 m/z 101.05 22.95% 27 - , — L , — H +49+ 1Tndn/DufTT 83 101 m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1 640: Morpholine. 4-methyl- 43

7.40 7.60 7.80 8.00 "T 5000 m/z 58.0,5 17.63% “ 15 101 27 71 56 TIaBUTTTT ' 1 ‘ i ■ 1 1 • i ■ • 1 1 i • • 1 1 i ■ • 1 1 I 1 1 ' ' 1 1 miz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone IT TT i । i rt t । T i TTTT ■ i i 43 7.40 7.60 7.80 8.00 m/z 41.05 7.25% 5000 58 27 — — 1 —4 T ‘ — 1 ■» « I » ' I ‘ ‘ i ‘ ' 1 i • 1 r 1 I 1 1r l 1 1 I 1 TIT ' ‘ TT - TTTTTPTF miz-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

25947.D NP103001.M Tue Dec 11 09:31:28 2001 Page 2

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