GCMS analysis results for sample AD26011, Dec 2001

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Data File : C:\HPCHEM\1\DATA\NOV2 001\26011.D Vial: 4 Acq On : 20 Nov 2001 3:31 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\l\METHQDS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration- Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.69 1.37 ug/1 251552 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Te ative ID MW MolForm ' CAS# Qual

1 2-Pentanone, -hydroxy-4-methyl- 116 C6H1202 000123-42-2 40 2 Acetone 58 C3H6O 000067-64-1 10 3 Morpholine 4-methyl- 101 C5H11NO 000109-02-4 9 4 3-Hydroxy -pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 288 (7.690 min): 26011 .D (-) m/ z 43.00 100.00% I 43

59 5000 101 TrrTrrmngrrr 7.40 7.60 7.80 8.00

m/z-> I ' ' ' ' I ' ' ' ' I 10 20 30 40 50 I--P 1-—3744 +53 71 83 m/z 59.0.5 49.54% 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43 - — । । 5000 59 7.40 7.60 7.80 8.00 m/z 101.05 2 2.74% 27 on 101 ■ i 49 I 83 | ■ ■ i ■ ■ ■ ■ i 1 ■ ■ I Id * I ' ••>!> ' । । | l ■ 14 111 l__ -------------

miz-> 10 20 30 40 50 60 70 80 90 100 110 'Abundance #62322: Acetone 43 7.40 7.60 7.80 8.00 I 5000 m/z 58.05 18.91%- i 58 l 27 • ■ । ■ n • • ■ । ■ ■ • ■ । • • ■ • । *18"-11111111T 'T _ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 43 7.40 7.60 7.80 8.00 m/z 41.05 7.07% 5000

15 101 71 NWN .... 1...... ■ ■ i 56 | —P - 1 1 >->—>-> | । । ' ' । m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

26011.D NP103001.M Tue Dec 11 09:22:44 2001 Page 1

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