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GCMS analysis results for sample AD26011, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26011 conducted on December 12, 2001.

NYC-WTC_000030895–000030906

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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Scanned page image, NYC-WTC_000030903
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2001\26011.D Vial: 4 Acq On : 20 Nov 2001 3:31 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Ethanol, 2-(2-ethoxyethoxy)- Concentration' Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.43 4.66 ug/1 857368 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanol, 2 -(2-ethoxyethoxy)- 134 C6H14O3 000111-90-0 2 2-Propanol, 1-(1-methylethoxy)- 118 C6H14O2 003944-36-3 45 3 Ethane, 1,1'-oxybis[2-ethoxy-] 162 C8H18O3 000112-36-7 38 4 Ethanol, 2-(2-methoxyethoxy)- 120 C5H12O3 000111-77-3 36 Abundance i Scan 695 (11.426 min): 26011.D (-) m/ z 45.05 100.00% 45

5000 59 72 11.00 11.20 11.40 11.60 11.80 —39l ----------- 1 1 • ■ । 89 104 . ' । ' 1 ' 1 । 1 . । .... TT . । । TT । ) । m/z 59.05 36.09% miz-> 20 30 40 50 60 70 80 90 100 110 120 (Abundance #65483: Ethanol, 2-(2-ethoxyethoxy)- 45

I 5000 i 31 59 11.00 11.20 11.40 11.60 11.80 72 m/z 72.00 28.19%

'm/z-> 1 I ■ ■ 20 30 ' ■ i ' ' ' ' i ■ ■ 1 ' i ' ' 1 ■ I ' ■ ‘ ' i 40 50 60 70 1 80 90 100 104 ... 110 116120, Abundance #3549: 2-Propanol, 1-(1-methylethoxy)- 45 I ' ' ' ' I ' 11.00 11.20 11.40 11.60 11.80 5000 59 m/ z 73.0P 14.54%- 31 73 88 103 I ' ' ' ' l ' ' ' 1 f ' i ' ' ' 1 i 1 * ' ' i '' ■ ' ■ I ' TT I 1 । m/z-> __ 20 30 ____ 40 50 60 70 80 90 100 110 120 Abundance #12866: Ethane, 1,1'-oxybis[2-ethoxy-] i ■ ■ ■ ■ i ■ ------ 11 45 11.00 11.20 11.40 11.60 11.80. m/ z 43 . OP 13.84% 59 5000 31 72

87 103 116

m/z-> ..... 20 —30....... 40 1 - 50 60 70 —————— 80 90 100 110 120 11.00 11.20 11.40 11.60 11.80

26011.D NP103001.M Tue Dec 11 09:22:49 2001 Page 2

NYC-WTC_000030903

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NYC-WTC_000030903Source: NYC Law Department, mirrored locally

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