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GCMS analysis summary, sample AD31403, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31403 showing surrogate recovery and unknown compounds from February 7, 2002.

NYC-WTC_000016260–000016271

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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Scanned page image, NYC-WTC_000016269
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1 502\31403.D Vial: 12 Acq On : 15 Jan 2002 9:43 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1,1'-[(1-methyl-l, Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.28 0.27 ug/1 59777 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1,1'-[(l-methyl-l,2-eth 192 C9H20O4 001638-16-0 59 2 2-Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 45 3 2-Propanol, 1-(2-ethoxypropoxy) - 162 C8H18O3 010143-32-5 39 4 3-Hexanol 102 C6H14O ______ 000623-37-0 38 Abundance 4 Scan 679 (11.277 min): 31403.D(-) m/z 59.05 100.00% 59

M 45 5000 73 103 11.00 11.20 11.40 11.60 ‘ I ‘ ‘ ‘ ' i ‘ ' i ■ lll|-----11 m/z 45.00 63.53% m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #20630:2-Propanol, 1,1'-[(1-methyl-1,2-ethanediyl)bis(oxy) 59

5000 — 11.00 11.20 11.40 11.60 31 45 103 m/z 73.00 5.72% 39 , ...... 73■ .................... ,L....... 117 i.,■• ■ i ■ ■ 1 ' i ■ ■ 1 ’'i 1 1 ' —4,1, ' i ■ ■ ■ ■ । *■ ■ • ‘ * ■ । ' ■ ■ । ।11 ■ । ■ •■■ m/z-> 20 30 40 50 ।60 70 80 90 100 110 120 Abundance 1108. 2-Propenol. 1.1oxbis 59 TTB1TTTTT 31 11.00 11.20 11.40 11.60 5000 45 m/z 103.05 28.02%

ANA 103

MJ 72 89 ' i • ■ ■ ' i ‘ ‘ • i • ' ■ i ■ ■ ■ ■ i ■ ■ ' ■ i ■ ■ ' 1 i ■ ' ■ i ■ ‘ ■ i ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #12860: 2-Propanol, 1-(2-ethoxypropoxy)- 59 11.00 11.20 11.40 11.60 m/z 45 5000 31 73 103

■ I ' ‘ ‘ I ' ' ' ' I ' ■ 1 ‘ I ■ ■ a01ji ..... A........ 1..... 116.. wWWw/ 1 I ‘ 1 ■ ■ i 1 ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 11.00 11.20 11.40 11.60

31403.D GCMS1126.M Mon Feb 04 15:11:38 2002 Page 3

NYC-WTC_000016269

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NYC-WTC_000016269Source: NYC Law Department, mirrored locally

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