GCMS analysis summary, sample AD31403, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\JAN1502\31403.D vial: 12 Acq On : 15 Jan 2002 9:43 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.59 0.71 ug/1 158364 1,4-Dichlorobenzene-d4 11.50

.Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propano: 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 83 2 2-Propano 1,1-dichloro­ 126 C3H4C12O 000513-88-2 10 3 1 - Fluorononane 146 C9H19F 000463-18-3 9 4 Decane, 1-fluoro- 160 C10H21F 000334-56-5 9 Abundance Scan 277 (7.587 min): 31403.D (-) m/z 4 .05 100.00% 43

5000-

—TTTnmnnnLmmTat 35 11 [11771 ,49 55 61 . * ,1 I, 174 83 97 , , ilp....... 11 117 125 7.20 7.40 7.60 7.80 8.00 1 1 1 I ' ’'1 1 1 1 m/z 124.85 10.64% 90 100 110 120 130 ' ■ i 1 ' • ■ i ■ ■ ■ ‘ i miz-> 10 20 30 40 50 60 70 80 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 ■ i ■ ■ ■ • i • 7.20 7.40 ..1^ .......... 7.60 7.80 8.00 15 m/ z 82.8.5 8.70% 35 ‘ .49 85 97 117 125 ‘■i1•■■i'1■‘i‘>i'111i1 ' 1 1 1 11 1 ■ I 1 1 1 1 1 1TH m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 368; 2-Propangne, 1, dichtoro- 43 MM... u.l, 7.20 7.40 7.60 7.80 8.00 5000 m/z 126.90 7.51% li 15 o= | 37 49 63 76 83 93 m/z-> Abundance • ■ i ■ ■ ‘ ■ i • ■ ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i • ■ • ■ i ■ ■ ■ • i • ■ • ■ i ■1 ■ ■ । 10 20 30 40 50 60 70 #8922: 1-Fluorononane 80 90 ■ i' • ■ ■ i ■ ■ • ■ i ■ ■ ■ ■ i ■ ■ 100 110 120 130 ।J. I 43 7.20 7.40 7.60 7.80 8.00 m/z 84.95 7.06%

M 5000 56 27 70 84 97 33 1 ■ ‘ i ■ ' 1 • i • ' ‘ ' i ‘ i ■ • i ‘ ‘ ■ i ■ ■ 1.44**14 • • । ■11 ■ ■ ■ ■ । ■ i • ■ ■ • i' • mlz~> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.20 7.40 7.60 7.80 8.00

31403.D GCMS1126.M Mon Feb 04 15:11:33 2002 Page 2

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