GCMS analysis results for sample AE00007, Feb 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2402\7.D Vial: 6 Acq On : 24 Jan 2002 5:57 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) - Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.58 0.66 ug/1 206679 1,4-Dichlorobenzene-d4 11.48

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 40 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 1-Fluorononane 146 C9H19F 000463-18-3 9 4 2 -Propanone, 'Abundance 1,1-dichloro- 43 Scan 276 (7.582 min): 7.D (-) 126 C3H4C120______ m/z 4 0 . 00% 000513-88-2 9

5000

7.20 7.40 7.60 7.80 8.00 1 1 । r '■'■'T' -44+ 37 ......... J;,.. 17 77, m/z 124.85 9.74% m/z-> 10 20 30 40 __ 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000- A , 7.20 7.40 7.60 7.80 8.00

15 m/ z 81.9.5 7.05% ...... I ' I ' ’ • ' I 1 35 49 85 97 117 125 ' ■ ' I ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4732: N-Acetyipyrrolidone 43 ------- 7.20 7.40 7.60 7.80 8.00 5000 m/z 96.9.5 6.71% 99 127 56 86 30 69 112 m/z-> ■ ■ i ■ ■ ' ■ i ' • ' ' I ■ ■ i 1 ■ ■ ' i ■ ■ ■ ■ i ■ 10 -20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8922: 1-Fluorononane .......... / ................... 43 7.20 7.40 7.60 7.80 8.00 m/ z 46.85 6.01%

m/z-> 5000

10 27

• ■ i ' ■ ■ ■ i ■ ■ ■ ■ i 20 30 33 ■ i 1 40 I TII 50 56

, I rV 60 70

70 80 84

90 97

100 110 120 130 AWwovha)

7.20 7.40 7.60 L—_ 7.80 8.00

7.D GCMS0208.M Fri Feb 08 13:41:18 2002 Page 2

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