GCMS analysis results for sample AD30354, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30354.D Vial: 6 Acq On : 27 Dec 2001 4:03 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.76 0.51 ug/1 187266 1,4-Dichlorobenzene-d4 11.68

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 43 2 N- Acetylpyrrolidone 127 C6H9NO2 000932-17-2 4 3 Hexadecanol 242 C16H340 029354-98-1 4 4 1-Fluorononane 146 C9H19F 000463-18-3 4 Abundance Scan 295 (7.755 min): 30354.D (-) m/z 4 .95 100.00% 43

5000

11/2/n///m/mknmm/nnn

m/z-> i 61 Tnpamnpontmmpnt84 97 .175...... TrrTTTTrrrpTTTTTTTTTTTrrpTTT^^ 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 7.40 7.60 7.80 8.00 m/z 124.85 10.17% Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 ........... Ha.......... 7.40 7.60 7.80 8.00 15 m/z 83.85 8.72%

mz-s 85 97 125 “0UIm—030—0Tpmmupumpmpgpu 10 2030405060 70 8090 100110120130140150160170180190 200 WWW/Uwwp Abundance #4 "32: N - Ace t yl pyrrolidone 43

7.40 7.60 7.80 8.00 5000 m/z 46.95 8.66% 99 127 86

mfe-> 30 mpmtm 56 69 112 . ।.... ।. i. t.... t. *.. t. i' TUu-0n—E0101—BM13101’0001301"1——3-1—1118 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 MWwA vww Abundance #32431: Hexadecanol ■ ' I ' ■ ' 1 i ' ■ ■ ■ i ' ■ ■ ■ i ■ ■ ■ ■ i ■ 43 7.40 7,60 7.80 8.00 m/z 96.90 6.56% 5000 27 68 82 56 96

miz-> ■ ■ i1' ■i‘1 ■ 1109.............................. 196 1.»1.। i i > 11 i 11 i 11 11111(i>11 • t i 111 i i ।>1111t i 11 । > i i i | i i 11|> *

10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 .7.40 '' 7.60 “ 7.80 A 8.00 ' ‘ '

30354.D GCMS1126.M Wed Jan 02 10:53:55 2002 Page 2

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