GCMS analysis results for sample AD30011, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC1801\30012.D Vial: 9 Acq On 18 Dec 2001 11:54 pm Operator: 209 GALOS Sample gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************************************************* ******************** Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.61 ug/1 164980 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 36 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 Ethyl Chloride 64 C2H5C1 000075-00-3 9 4 Ethanol, 2,2,2-trichloro -__ 148 C2H3C130___ __ 000115-20-8 9 'Abundance < Scan 294 (7.745 min): 30012.D (-) m/ z 42.95 100.00% 43

5000-

Id1/d/d/d/d1n/—1—E11111 35 7.40 7.60 7.80 8.00 — r । — r , , --+ 49,5563...... 83..... 97,103—119117 TIIunr I ] 1 i ■ । | - i < I | 111 ' | ‘ 11 ' ' 1 • I' ' ' 1 | 1 ’II 1 m/z 124.85 11.29% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000- ■ i ■ ■ ■ ■ i 1 7.40 7.60 7.80 8.00 m/z 35.00 8.65% 15 I 35 49 85 97 117 125 ’rTT I I l t I 1 I I I I I » I I 111 I I • A m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone | 43 740 7.60 7.80 8.00______ 5000 m/z 96.95 8.37% 99 127 56 86 30 69 ill , 112 • i • ■ • ■ । ■ • ■ • । • ' I ' ' • ' I ' 1 1 'I 11 I 1 I 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #62380: Ethyl Chloride TICCLLILn/O.k. 29 7.40 7.60 7.80 8.00 m/z 126.90 7.87% 64 5000 49 35

m/z-> ' • i • ■ ■ ■ i ■ ■ ■ ■ i ■

10 20 30 1. ■ ■ ' i ■ ■

40 Jr50. 60 'll..70- 80 90 100 110 120 130 7.40 7.60 7.80 • • i > • ■ ■ i • 8.00

30012.D GCMS1126.M Tue Jan 15 15:32:32 2002 Page 2

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