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GCMS analysis results for sample AD31404, Feb 2002

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Laboratory report documenting GCMS analysis of sample AD31404 conducted on February 13, 2002.

NYC-WTC_000018343–000018352

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31404.D Vial: 9 Acq On : 16 Jan 2002 7:27 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.59 0.89 ug/1 205321 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 42 23 Ethanol, 1-Octadecanol 2,2,2-trichloro- 270 C18H380 000112-92-5 9 148 C2H3C130 000115-20-8 9 4 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 7 Abundance Scan 277 (7.588 mln): 31404.D (-) m/z 43.05 100.00% 43

5000 1 i ' ' ■ ■ I1 1 1 1 1 1 1 1 1 I ' 1 1 ‘"1 1 1 64 82 97 125 7.20 7.40 7.60 7.80 8.00 | ■ > H ‘ ‘ ri" V. 60°.._I, ..I. ....... . 80 166 120 140 160 180 200 220 240 260 m/z 124.95 9.22% miz-> 20 40 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 ■ i ' ■ ‘ ■ i ‘ ■ 4 i ■ ■ • ' i ■ ■ • ■ i ' 1 7.20 7.40 7.60 7.80 8.00 15 m/z 96.9,5 7.57% I 85 97 125 * * i • '' i f 111 111 It 1 • ■ 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance £72027 1 -etadccano; 43 7.20 7.40 7.60 7.80 8.00 5000 82 m/z 46.95 7.51% 56 68 97 i < 111 125 224 270 m/z-> ' 20 40 60 80 100 120 140 160 180 ‘266' '226' '246' 266' Abundance #9118: Ethanol, 2,2,2-trichloro- 31 7.20 7.40 7.60 7.80 8.66 ‘ m/z 127.00 7.24% 5000 49 77 113 -------------------- miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 7.20 7.40 7.60 7.80 8.00

31404.D GCMS0103.M Thu Feb 07 09:13:17 2002 Page 2

NYC-WTC_000018351

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NYC-WTC_000018351Source: NYC Law Department, mirrored locally

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