Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
NYC-WTC_000035978–000035989Folder label: “GCMS X 11/30/01 A 12/11/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29026.D Vial: 30 Acq On : 11 Dec 2001 4:58 pm Operator: 209 GALOS Sample : gc/ms scan 11/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
7.75 0.59 ug/1 148520 1,4-Dichlorobenzene-d4 11.67
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 50 2 Ethanol, 2,2,2-trichloro- 148 C2H3C130 000115-20-8 12 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 4 2-Propano: , 1,1-dichloro- 126 C3H4C120_____ 000513-88-2 9 Abundance Scan 294 (7.746 min): 29026.D (-) m/z 4 .05 100.00% 43
5000
miz- 36 .. .'i.,i ।. 55 36 ’ 1’11117 TI 63 r. T ’’1’ 11 „ 83 75,4 ■' i • ■ ■ • i' ■ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 99 117 127 II. । —011010/1’1 .! ।..»• m/z TTTTIInuu TTTIr i . . i । > 7.40 7.60 7.80 8.00 82.95 9.73% Abundance #12247:2-Propanone, 1,1,1-trichloro- 43 !
5000 AAALAA. 7.40 m/z 126.90 7.60 7.80 8.00 8.57% 15 | 35 85 97 117 125 ’ 1Trrrp-rrry —PmmTT T’T TTTTUgmT miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66530: Ethanol. 2,2,2-trichforo- 31 • • i > ■ ■ ‘ i ■ • • ■ T •1 ■ ■ i ' ■ ■ ■ i 1 7.40 7.60 7.80 8.00 5000: m/z 124.90 8.34% 49 77 84 . TTIInuuuou—m’—’I’ TInpu 95 113 121 T 150 11’3 I * ‘' * I * I T miz-> 1020 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance” #4732: N-Acetylpyrrolidone ' 1 I 1 ‘ 1 ‘ 1' 1 । | I : i i । i i 1111 43 7.40 7.60 7.80 8.00 m/z 81.95 7.75% 5000 99 127 30 . 56 86 69......Ill , , 112 tTjT-m-j’’’’1’18Tyr’ 111’II1TT TTTIam TCpan—nm—anpmuUpuT T I TT T I TT TBnn i i i T । t r T I । j miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 7.40 7.60 7.80 8.00
29026.D GCMS1126.M Wed Dec 12 15:46:48 2001 Page 2
NYC-WTC_000035986
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NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035955
Laboratory report documenting GCMS scan results for sample AD29137 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035808
Laboratory analysis notes for sample AD29023 indicating no unusual compounds detected in GCMS scan; one of forty-three compounds in quality control standard outside acceptance rang
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035919
Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036079
Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000035888
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000035889
Fragmented laboratory data sheet recording sample volumes and drip rates for GCMS Method S08 analysis.
Filed in the same folder
NYC-WTC_000035890
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
Filed in the same folder
NYC-WTC_000035900
Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.
Filed in the same folder
NYC-WTC_000035904
Document containing reference values and recovery data for organic compounds analyzed by GCMS.
Filed in the same folder