GCMS analysis comments, sample AD29026, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29026.D Vial: 30 Acq On : 11 Dec 2001 4:58 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Misc. Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.64 ug/1 161804 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual l 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H1603 020324-32-7 83 2 1-Propanol ,/2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 3 2-Butanol,3,3’-oxybis- 162 C8H18O3 054305-61-2 50 4 2 - Pentanou., 2-methyl - 102 C6H140 000590-36-3 42 Abundance Scan 686 (11.344 mln): 29026.D (-) m/z 59.05 100.. 00% 59

5000 45 103 73 ‘itI 11.00 11.20 11.40 11.60

miz-> 20 —.—4— -Ht 30 40 50) 60 70 ■ । 80 86 । ■ 90 — yr-m TEtEITT "211/8 100 110 120 130 140 m/z 44.95 48.42% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59 5000 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 33.89% > l ■ ■ • 'T ' ‘ ■ 1 I 1 —I II । 130 । —r II . । > । ।........... miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #5086: 1-Propanol 2-{2-hydroxypropoxy)- 59 * * 1 * 11.00 11,20 11.40 11,60 5000 m/ z 73.00 27.25%

NA 31 45 103

75 89 -IPPIT i । » i » i । t । । । j । । । » । r rirj TTnI i i < i j i t i i । i miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859:2-Butanol, 3,3‘-oxybis- TTIBTPLT 59 11.00 11.20 11.40 11.60 m/z 41.05 — 25.78% 5000 31 45 103

—I — IT . — TI1r — ITr IBumpun -rr II r .l_______________ 134 i i j > V 4 i J : t t' l | I I l 1I8

m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 _ 11-00 11-20 11.40 11.60

29026.D GCMS1126.M Wed Dec 12 15:46:53 2001 Page 3

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