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GCMS analysis results sample AD29459, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29459 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036447–000036457

Folder label: “GCMS X 12/5/01 A 12/12/01

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Scanned page image, NYC-WTC_000036456
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1201\29459.D Vial: 26 Acq On : 13 Dec 2001 3:21 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.42 1.01 ug/1 263427 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol ,/l-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol / 3,31-oxybis- 162 C8H18O3 054305-61-2 64 3 1-Propanol, 2- (2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 53 4 2-Propanol, 1-(2-methoxypropoxy) - 148 C7H1603 013429-07-7 47 Abundance Scan 695 (11.421 min): 29459.D (-) m/z 59.05 100.00% I I 59

5000 45 103 M 45 . X 0 73

-A—— ■ 1 । ■ ■ ■ ■ । 11.00 11.20 11.40 11.60 11.80 -- • । > ■ ■ • । ■ TH m/ z miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 103 11.00 11.20 11.40 11.60 11.80 73

m/z-> 20 .. L 31

30___ 40 50 —mm TT T 60 70 80 90 100 110 120 130 130 140 m/z 103.05 36.40%

Abundance #12859: 2-Butanol, 3.3-oxybis- 59 TT 11.00 11.20 11.40 11.60 11.80 5000 31 m/ z 73.00 26.88%

NA 45 103

I i 134 ' i ' ' ' ' i ' ' ' ' i ' ' ' ' i ' ■ ' ' i ' ' ■ ' i ' ' 1 ■ i ' 1 ' ' i ■ ' 1 1 i 1 1 ‘ 1 1 1 ri"' I । । । । । । । । । । । 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- Ttr T ' । ’ । I l-'-| । I 1 । 59 11.00 11.20 11.40 11.60 11.80 m/z 41.00 21.53% 5000-

m/z-> 20 30 31

40 45

50 HT ' i ' 75 I60 89 103

' ' • i ' ' ' ' i ' ' ' ' I ' 1 ' ' i 1 ' • ■ I ■ ■ • 1 i 1 • • ’ i ■ 70 80 90 100 110 120 130 140 11.00 A 11.20 11.40 11.60 11.80

29459.D GCMS1126.M Fri Dec 21 12:26:33 2001 Page 3

NYC-WTC_000036456

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NYC-WTC_000036456Source: NYC Law Department, mirrored locally

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