GCMS analysis results sample AD29459, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1201\29459.D Vial: 26 Acq On 13 Dec 2001 3:21 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.35 0.71 ug/1 186416 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative* ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3,3' -xybis- 162 C8H18O3 054305-61-2 50 3 2-Pentanone, 5-methoxy- 116 C6H12O2 017429-04-8 45 4 Ethane, 1-ethoxy- l -methoxy- 104 C5H12O2 010471-14-4 45 'Abundance Scan 687 (11.348 min): 29459.D (-) m/z 59.05 10 . 00% i 59 ii

5000- 45

aL51——— TT+ 73

86 1 ■ ■ i ■ ' 1 ' i ' ■ ' ■ i 103

, । ■ ■ ■ • । • ■ ■ • । • • ■ ■ । ■ 11.00 m/ z _N 11.20 11.40 11.60 45.00. 53.55% ■ ■ i ’

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

□ 5000 11 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.0537.61% —. — , . । 130 m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3‘-oxybis- 59 ' I ' ' »'(■••• I f 11.00 11.20 11.40 11.60 5000 31 m/ Z 73.00 30.89% 45 103

l i 134 TOtr"1"1/LICC-I/I-/TII—"Ld/I/T/IIIECI-ITCCnIIDII/I/I-T-T TTIv 1 ' । i । m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #64282: 2-Pentanone, 5-methoxy- TI1 • । < ■ ■ ■ । 1 > ■ > । ■ 1 > i ■ 43 59 11.00 11.20 11.40 11.60 m/ z 41.05, 27.93% 5000 -

69 ..... 1 , ' I ’ ' ' ' I ' ’ ' ' I ' * 1 , 84 101 116 I ' ' ‘ ' i ' ' ' ' i ' ' ' ' i ' ' ' ' I 1 1 1 ' | । 1 > 1 | > > i" 1 | । 1 1 1 | 1 TIT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

29459.D GCMS1126.M Fri Dec 21 12:26:28 2001 Page 2

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