GCMS analysis results for sample AD30011, Jan 2002

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Gas chromatography-mass spectrometry report documenting analysis of sample AD30011 conducted on January 28, 2002.

NYC-WTC_000037314–000037326

Folder label: “GCMS X 12/11/01 A 12/18/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\30012.D Vial: 9 Acq On : 18 Dec 2001 11:54 pm Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.35 0.43 ug/1 115322 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1—C2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 64 3 1-Propanol, 2-(2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 42 4 2-Propanol, Abundance C -oxybis- 1,1'Scan ____ ;___ 134 C6H14O3 687 (11.352 min): 30012.D (-) 000110-98-5 42 m/z 59.00 100.00% 59

5000

■ । ■''' । • — 45

r 51 73

83 103

। ■ i■ ■ > > ■।■•■■।■",,(। ( । . "I 11.00 m/z 11.20 45.00 N 11.40 11.60 47.98% IT

m/z-> 20 30 40 !50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 - 45 103 1 । 1 1 1 I—r 1 । 1 1 TT 73 11.00 11.20 11.40 11.60 31 m/z 103.00 29.26% ------------- —PT TIT .-|> । i < । i ।......... 130.... m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3°-oxybis- 59i 11.00 £ 2...................... 11.20 11.40 11.60 5000 31 m/ z 73.00 25.95%

AN 45 103 I i l _____ |_______________ ..............134 ’I ’ TTr '“I”1 ■ i ■ ■ ■ ■ I • ' ■ ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■ ■

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- r ■ I ‘ Tr ' ' i ' 59 11.00 11.20 11.40 11.60

; NA m/z 41.05 23.33: 23.05% 5000 31 45 .103

-IP+. ,.... 75.... 89 11'' ■' i ■' • ■ i ■r' ■ i ■ ■ ■' i •1 •11'1111 >1 r1 > i • ।1 CMPPr - m/z-> 20 30 40 50 I60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

30012.D GCMS1126.M Tue Jan 15 15:32:37 2002 Page 3

NYC-WTC_000037323

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NYC-WTC_000037323Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AD30014, Jan 2002 · Box DEP Box 22

NYC-WTC_000037301

Gas chromatography-mass spectrometry report documenting analysis of sample AD30014 conducted on January 28, 2002.

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