GCMS analysis results for sample AD29926, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1801\29932.D Vial: 16 Acq On 19 Dec 2001 6:44 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 1.17 ug/1 325883 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative*ID MW MolForm CAS# Qual 1 2-Propanol, 1- ( methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3,31 -oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propano1, 1,1'-oxybis- 134 C6H14O3 000110-98-5 56 4 1- Propano 1, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Abundance Scan 695 (11.428 min): 29932.D (-) m/z 59.05 100.00% 59

5000

rl51—— 45 73

89 TTt +‘T-rT-r-|-r-rT-r 103 N I ' ' ' ' I ' ' 1 ' I ' ' ‘ ' I ' 11.00 11.20 11.40 11.60 11.80 m/z 45.05 • ■ i ■ ■

47.59% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-meihoxy-1-methylethoxy)- 59

5000 / 1 * I 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/ Z 103.00 36.25% —P- — ■ ■ ■ ■ ।1 ............... ।................ 130 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3°-oxybis- 59 — 11.20 11.00 A 11.40 11.60 11.80 "Ir . , , । r-r-r-^-T-r

NA 5000 31 45 m/ Z 73.00 28.13% 103

‘i"_____ , . .-p_______ 1 -........ i . . • 1′1 ....... 134 m/z-? 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1'-oxybis- 59 11.00 11.20 11.40 11.60 11.80 m/ z 41.05 25.46% 31 5000 45

103 89 > । > ■ ■ ■ । ■ 11 — —— H ' ।721 ' 1 ' i * 1 1 * । 1 ■ * ■ । Tr I ................... । . । । । | r r. । | i m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

29932.D GCMS1126.M Tue Jan 15 15:26:17 2002 Page 3

NYC-WTC_000037361