GCMS sample analysis AD29285, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1201\29293.D Vial: 14 Acq On : 12 Dec 2001 3:40 pm Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.42 1.07 ug/1 283477 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy- l -methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1,1/ - oxybi s- 134 C6H14O3 000110-98-5 56 3 2-Butanol, 3,3 -oxybis- 162 C8H18O3 054305-61-2 50 4 2-Propanol, 1- (2-methoxypropoxy) - Abundance

m/z-> 5000

Abundance 20__ 30 40 /

45

39, 51 1 1 TI ' i ' 50 Scan 695 (11.425 min): 29293.D (-)

—. + 60 59

#9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59 70 80 73

90 88............... ।............................................... 100 110 120 103 148 C7H16O3

130 140 ____ 013429-07-7 50 m/z 59.05 100.00%|

11.00 m/z A 11.20 11.40 44.9.5 11.60 11.80 49.22%

5000 - r■ 4 । • 1 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.05 35.57% PPPH —T .............................. ।........................... 130............ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1-oxybis- 59 --------

A 11.00 11.20 11.40 11.60 11.80 31 5000 45 m/z 73 00 25.71% 103 89 I • i ■ ■ • • i • ! I ' I ' ' 72 1 i ' ' ' ' I ' ' ' ' i ■ ' ■ ■ i ' ) m/z--> 20 30 40 50 60 70 80 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3'-oxybis- 59 11.00 11.20 11.40 11.60 11.80 m/z 41.05 23.70%

VA 5000 - 31 45 103

- । । j --- 134 1 I ' ' 1 ' i TT 1 1 1 1 —TTTTT TUT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

29293.D GCMS1126.M Fri Dec 28 15:24:37 2001 Page 4

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