GCMS sample analysis AD29285, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC1201\29293.D Vial: 14 Acq On 12 Dec 2001 3:40 pm Operator: 209 GALOS Sample gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.76 ug/1 202563 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2/4nethoxy-1-methylet 148 C7H1603 020324-32-7 90 2 1-Propanol, 2-(/-hydroxypropoxy) - 134 C6H14O3 000106-62-7 59 3 2-Propanol, 1,‘-oxybis- 134 C6H14O3 000110-98-5 56 4 2-Butanol, 3 ,/3 ' -oxybis- 162 C8H18O3 054305-61-2 50 Abundance ’ Scan 686 (11.342 min): 29293.D (-) m/ z

M 59.05 100.00% 59

5000 45 73 103

39 ,i 11.00 11.20 11.40 11.60 —.... - 84 130 ■ 1 i ' THt t1I TT +4 m/ z 45.05. 45.52% m/z-> 30 40 50 60 70 80 90 100 110 120 130 'Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 , — 4 -4 — , — 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 • 34.72% - I I I-PI-T -III 130 m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 50 - p 11.00 11.20 11.40 11.60

A 5000 m/z 73.00 28.10% 31 45 103

il 75 ■ 89 । ■ ' i ' ' ■' । ‘ । ■ 1 । ■ TTT । । >i । । । । T-r-f-rr-r-r-p-,-, TIur , m/z-> 30 40 50 60 70 80 90 1G0 110 120 130 Abundance #6087: 2-Propanol, 1,1-oxybis- 59 _11.00 11.20 11.40 11.60 _ m/z 41.05, 23.09% 31 5000 - 45 103 89 72 ——— I' ' ■ ' i 1 ' ' ' i ' ■ ' ■ I i 1 ' ‘ ' i TT III.T 1 ■ i 1 1 ■ i_r~' fTr 1 1 ’ I ' 1 1 1 I ' 1 1 ' I m/z-> 30 40 50 160 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

29293.D GCMS1126.M Fri Dec 28 15:24:32 2001 Page 3

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