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GCMS sample analysis AD29285, Dec 2001

Machine-extracted title · confidence 95%

Laboratory analysis report for sample AD29285 conducted on December 28, 2001, including surrogate recovery data.

NYC-WTC_000036311–000036324

Folder label: “GCMS X 12/4/01 A 12/10/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC12 01\2 92 93 . D vial: 14 Acq On 12 Dec 2001 3:40 pm Operator: 209 GALOS Sample gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.55 ug/1 146242 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 56 2 2-Pentene, 2-methoxy- 100 C6H120 061142-47-0 9 3 Octadecane,/l-(ethenyloxy)- 296 C20H40O 000930-02-9 9 4 Ethanol, 2/2,2 - trichloro- 148 C2H3C130______ 000115-20-8 9 Abundance Scan 294 (7.744 min): 29293.D (-) m/z 4 . 05 100.00%| 43

5000-

. > j । । rr । ... । । . n i . । । ।

63 83 97 125 7.40 7.60 7.80 8.00 m/z 124.95 8.40% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000- 7.40 7.60 1 7.80 ■ ■ i • ■ • • । 3.00___ __ 15 m/ z 82.85 6.44% | 85 99 125 •1 I • TITI I'' ' ■ f T’T l' ■1 ■ i T‘ m/z—> 20 40 60 80 100 120 140 160 180 20 220 240 260 280 300 Abundance #1570: 2-Pentene, 2-methoxy- 43 72 . 85 MAAA. ‘II । 7,40 7.60 7.80 8.00 5000- 100 m/z 126.90 5.92% 59

TITITrIIIr1‘I11‘tT‘E‘rI"‘111111111EETT"E"‘T-‘TTTT‘11‘‘1IVITTCTTTTT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42184: Octadecane, 1 -(ethenyloxy)- ■ i ■ ■ ■ ' i 43 57 7.40 7.60 7.80 8.00 m/ z 96.85 5.64% 5000- 83 27 75 97

m/z-> ■ • t ■ ■ • ■ i ■ •

20 40 — 60 80 | 111 4 | 278 296 100 120 140 160 180 200 220 240 260 280 300 17.40 7.60 • I ■ • ■ ■ l..... i 7.80 8.00

29293.D GCMS1126.M Fri Dec 28 15:24:28 2001 Page 2

NYC-WTC_000036319

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NYC-WTC_000036319Source: NYC Law Department, mirrored locally

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