GCMS sample analysis AD29285, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\29293.D Vial: 14 Acq On 12 Dec 2001 3:40 pm Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.87 ug/1 1026290 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1,3 -Dipxolane , 2-methyl- 88 C4H802 000497-26-7 9 3 1,3 -Dioxolane , 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Sila: , tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 278 (7.597 min): 29293.D (-) m/z 73.0.0 100.00% i i 73

5000 43 87 103 7.20 7.40 7.60 7.80 8.00 , | 50 55 60 67, । , • 1 r1 I 1 1 i 1 ' । ' r' ' ' ■ i ' ■ i ■ ■ ■ ' i ''■ ■ ■ i ■ ■ ■ ■ i ' ■ m/z 43.05 26.01% miz->10 20 30 401 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73

5000 44 58 7.20 7.40 7.60 7.80 8.00 m/ z 44.95 10.13% r 15 .1 —+ — I ' ' 1 ' I ' 1 ' ' I ' ' 1 ' I ' ' 1 1 I 1 11 1 rT 1 1 1 1 1 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62902: 1,3-Dioxolane, 2-methyl- 73

7.20 7.40 7.60 7.80 8.00 5000 - 43 m/z 41.00 9.84% 58 27 I 87 | I — ——————— m/z-> 10 20 30 40 50 60 70 80 90 0( 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet Tr —r i T — IEn—mmn 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.79%

m/z-> 5000-

1 i ■ ' ' ' i ' 10 20 ' । 30 36 ■ 1 ■ 40 45

■ ■ । •1 50 55 67, ।' । ■ TT 1 4-r 60 70 ............ 109 115 . 80 90 100 110 120 7.20 7.40 L 7.60 7.80 8.00

29293.D GCMS1126.M Fri Dec 28 15:24:24 2001 Page 1

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