GCMS sample analysis AD29291, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29235.D Vial: 8 Acq On : 12 Dec 2001 6:34 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 4.03 ug/1 1030330 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformami 73 C3H7NO 000627-45-2 9 2 Silane, tetrai thyl- 88 C4H12Si 000075-76-3 9 3 1,3 -Dioxolane , 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1 - But anamine, 3 -methyl - 87 C5H13N 000107-85-7 7 ‘Abundance Scan 279 (7.603 min): 29235.D (-) m/z 73.00 100.00% 73

5000 43 87 103 7.20 7.40 7.60 7.80 8.00

miz-? — 10 . - 20 -34 30 40 , 1 50 55 PTmPI 50_60 67, । +r 70 80__ 90 ■ i 1 • * 1 i ■ ' ‘ 1 i ■ ' 1 ' i 1 ' ‘ 1 1 1 ' 100__110__ 120 m/z 43.00 26.02% Abundance 310 #292: N-Ethylformamide 73

5000 58 7.20 7.40 7.60 7.80 8.00 44 m/z 44.95 9.85% —1 Im I . I I I I 1 l 4 . I . . . I I , . I I ( . I I . j l I . k I I . miz-> 10 20___ 30 40 50 60 70 80 90 100 110 120 Abundance #62932, Sitane, tetramethyl- 73 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.00 9.49%

45 15 k । । . । । i । i 53 59 88 1 1 • 1 ■ ‘ i 1 1 1 ‘ I ‘ ‘ 1 1 i ' 1 1 ‘ i ‘ 1 1 1 I ■ ' ' 1 ) ‘ ' 1 1 i ' 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423:1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet TTTrTmmTPTrr 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.83% 5000

miz-> 36 i I 45 55 67, —p TTr TTn.rrmrittr 4r ■ i ■ ■ ■ ■ i ■11 ‘ i1 ■ • 109 10 20 30 40 50 60 70 80 90 115 • i1 • •11 • ‘ 100 110 120 7.20 7.40 L n 1 1 1 1 ' I 1 1 • ‘ 1 1 ' ' ' I > ‘ ‘ 1 1 1 • 7.60 7.80 8.00

29235.D GCMS1126.M Wed Dec 19 12:53:04 2001 Page 1

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