Laboratory analysis report for sample AD29291 conducted on December 28, 2001, including surrogate recovery data.
NYC-WTC_000036232–000036242Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal D. ocument
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC1001\29235.D Vial: 8 Acq On : 12 Dec 2001 6:34 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
11.35 0.72 ug/1 183997 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanol, 1- (2-methoxy- 1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1,11 -oxybis- 134 C6H14O3 000110-98-5 56 4 2-Propanol, 1-( 2 -methoxypropoxy) - 148 C7H16O3 013429-07-7 47 Abundance 7 Scan 687 (11.348 min): 29235.D (-) m/z 59.05 100 .00% $
miz-> 5000
‘ i11 • * j'1 20 30 91— — 40 45
501 60 73
— V' 1 I ' 1 ' 89 70 80 । 103
1 1 < i । । j i H i ( । 90 100 110 ‘ | i < - 1 1 i • ■ ■ | i 120 130 140 11.00 11.20 11.40 11.60 m/ z .N 45.05. 50.44% 11 ( '
Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59
5000 103 TT 19 T i i Il Infill T I I 45 73 11.00 11.20 11.40 11.60 31 m/z 103.05. 34.12%
m/z~> Abundance
5000 20 — 30T -I 40 TOTT 11 1 1IIT ii । 50
31 60 70 80 90
45 100 110 120 130 140 412859. 2-Butano!, 3.3‘-oxybis- 59 130
............ — 11.00 11.20 11.40 11.60 m/z 73.00 W 28.79%
NA 103
... ....... I...... ,................. TLTTCCTTCCI1TTT2112TT5ST*TrT ........... 134 ‘‘T-TTTTI1-1-1111110TrIT miz-> 20__ 30 40 50 60 __ 70__ 80__ 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,T-oxybis- 59 11.00 11.20 1140 iteo' 77 m/z 41.05 23.46% 31
UN 5000 45 103 89 72 * TIBp —1 frtrr TIr 1 I ' 1 ‘ 1 1 J 1 ' ■ I ' ' 1 1 I ' miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60
29235.D GCMS1126.M Wed Dec 19 12:53:09 2001 Page 2 NYC-WTC_000036240
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035820
Lab notes for sample AD29022 indicate no unusual compounds detected but one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036267
Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036480
Laboratory report documenting GCMS analysis of sample AD29462 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036380
Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
Filed in the same folder
NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
Filed in the same folder
NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
Filed in the same folder
NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
Filed in the same folder