Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.
NYC-WTC_000036079–000036091Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC1001\29234.D Vial: 23 Acq On : 11 Dec 2001 8:10 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
11.41 5.66 ug/1 1416600 1,4-Dichlorobenzene-d4 11.68
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H1603 * 020324-32-7 72 2 2-Butanol, 3,3’-oxybis- 162 C8H18O3 054305-61-2 50 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 4 2-Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 40 Abundance Scan 693 (11.409 mln): 29234.D (-) m/z59.05 100.00% 59
5000
....... 32153— — 45
85 91 TIT TITTIT । 1 TTTT ( 130 । 73
। . m/z 44 0 45.85% 103 T A J* • *'I • 11 1 PPP r 11.00 11.20 11.40 11.60 11.80
mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy}- 59
5000 45 103 N 11.00 11.20 11.40 11.60 11.80 31 73 m/z "7 35.22% ........................ [ _ ................130......... —IP 80 90 100 110 1120 130 140 mfz~> 20 30 40 50 60 70 undance #12859: 2-Butanol, 3,3°-oxybis- 59 i » । » i 11119SI j I i 11.00 11.20 11.40 11.60 11.80 5000 31 45 m/z 73.00 27.01% 103
11117111 _ 1O00m2/*ttT117-11-r1711111**111111*1**1111‘S115134 ‘‘113 miz—> 20 30 40__ 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 1.B T I » J I I : T[ T T 3 T T 1181 59 11.00 11.20 11.40 11.60 11.80 m/z 41.05 23.01% 5000
miz-> 30 31
40 45
—PPP +— ' I ‘ TT I"1 1 " I ■ 75 20 50 60 70 ''“1 80 89 «"i > > ‘ ' | • 1 I T 1on/n.m I I I I I I I J I > I I 90 100 103
110 120 130 140 T r-rt-fT NUA 11.00 11.20 11.40 11.60 11.80
29234.D GCMS1126.M Fri Dec 14 16:48:47 2001 Page 5
NYC-WTC_000036090
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NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035955
Laboratory report documenting GCMS scan results for sample AD29137 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035808
Laboratory analysis notes for sample AD29023 indicating no unusual compounds detected in GCMS scan; one of forty-three compounds in quality control standard outside acceptance rang
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035919
Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
Filed in the same folder
NYC-WTC_000036044
Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
Filed in the same folder
NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
Filed in the same folder
NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
Filed in the same folder